Analytical Chemistry

Major: Industrial Pharmacy
Code of subject: 7.226.02.O.007
Credits: 7.00
Department: Physical, Analytical and General Chemistry
Lecturer: assoc. prof. Marta LARUK
Semester: 1 семестр
Mode of study: денна
Мета вивчення дисципліни: to provide students with theoretical knowledge of analytical chemistry and instrumental methods of analysis and to familiarise them with methods of qualitative and quantitative determination of the composition of substances.
Завдання: General: - Ability to assess and ensure the quality of work performed. professional: - ability to implement all stages of pharmaceutical development of medicines and draw up the results of drug development and research in the format of materials of the registration dossier; - ability to conduct stability studies of medicinal products and perform measures for proper storage of medicinal products during their industrial in their industrial production.
Learning outcomes: As a result of studying the discipline, the student should be able to demonstrate the following learning outcomes: Know - basic principles of analytical chemistry as a science of qualitative and quantitative composition of substances; - conditions for analytical determinations; - algorithms for creating new methods of analytical control of substances. Be able to - reproduce analytical methods from the description; - evaluate the metrological characteristics of the analysis results; - use laboratory equipment and instruments for to determine the content of substances.
Required prior and related subjects: Previous academic disciplines: - General and inorganic chemistry - Organic chemistry - Physical and colloidal chemistry Related and subsequent subjects: - Quality control of medicines - Pharmacognosy - Physical methods of drug analysis
Summary of the subject: Analytical chemistry provides information on substances' qualitative and quantitative composition using chemical (titrimetric and gravimetric) and physicochemical (optical, electrochemical, chromatographic) analysis methods. This enables technological processes in food and other industries to be carried out based on data on the content of certain substances in raw materials, finished products, the environment, water, etc. The discipline is studied by combining a theoretical course and laboratory classes on specific methods and objects of analysis.
Опис: - Subject, tasks, basic concepts and classification of methods of analytical chemistry. - Physical and chemical methods of analysis. - Molecular absorption analysis. - Chromatographic methods of analysis. - Electrochemical methods of analysis. - Conductance and coulometry. - Voltammetry.
Assessment methods and criteria: Form of semester control - differentiated credit; forms of current forms of current control: written and oral control, colloquia, defence of control works, defence of laboratory work, test control.
Критерії оцінювання результатів навчання: Points and grades are assigned by the Regulations on the organisation and semester control of students' learning outcomes developed by the Law of Ukraine “On Higher Education”, the Statute of Lviv Polytechnic National University, the Regulations on the organisation of the educational process at Lviv Polytechnic National University and other applicable legislative and regulatory documents on the organisation of the educational process.
Порядок та критерії виставляння балів та оцінок: 100–88 points – (“excellent”) is awarded for a high level of knowledge (some inaccuracies are allowed) of the educational material of the component contained in the main and additional recommended literary sources, the ability to analyze the phenomena being studied in their interrelationship and development, clearly, succinctly, logically, consistently answer the questions, the ability to apply theoretical provisions when solving practical problems; 87–71 points – (“good”) is awarded for a generally correct understanding of the educational material of the component, including calculations, reasoned answers to the questions posed, which, however, contain certain (insignificant) shortcomings, for the ability to apply theoretical provisions when solving practical tasks; 70 – 50 points – (“satisfactory”) awarded for weak knowledge of the component’s educational material, inaccurate or poorly reasoned answers, with a violation of the sequence of presentation, for weak application of theoretical provisions when solving practical problems; 49-26 points - ("not certified" with the possibility of retaking the semester control) is awarded for ignorance of a significant part of the educational material of the component, significant errors in answering questions, inability to apply theoretical provisions when solving practical problems; 25-00 points - ("unsatisfactory" with mandatory re-study) is awarded for ignorance of a significant part of the educational material of the component, significant errors in answering questions, inability to navigate when solving practical problems, ignorance of the main fundamental provisions.
Recommended books: 1. ENMK «Analitychna khimiia» https://vns.lpnu.ua/user/index.php?id=17319 2. Marta Laruk, Analitychna khimiia ta fizyko-khimichni metody analizu: navch.posibn. Lviv: SPOLOM , 2023.- 304 s. 3. Analitychna khimiia (khimichni metody analizu). M.M. Laruk, P.I. Shapoval, V.Ie. Stadnik. Lviv, Vydavnytstvo «Tarasa Soroky», 2022.-247 s.
Уніфікований додаток: Lviv Polytechnic National University ensures the realization of the right of persons with disabilities to obtain higher education. Inclusive educational services are provided by the Service of accessibility to learning opportunities "Without restrictions", the purpose of which is to provide permanent individual support for the educational process of students with disabilities and chronic diseases. An important tool for the implementation of the inclusive educational policy at the University is the Program for improving the qualifications of scientific and pedagogical workers and educational and support staff in the field of social inclusion and inclusive education. Contact at: St. Karpinsky, 2/4, 1st floor, room 112 E-mail: nolimits@lpnu.ua Websites: https://lpnu.ua/nolimits https://lpnu.ua/integration
Академічна доброчесність: The policy regarding the academic integrity of the participants of the educational process is formed on the basis of compliance with the principles of academic integrity, taking into account the norms "Regulations on academic integrity at the Lviv Polytechnic National University" (approved by the academic council of the university on June 20, 2017, protocol No. 35).