Design of Organic Synthesis Processes

Major: Chemical Technology and Engineering
Code of subject: 6.161.12.E.077
Credits: 6.00
Department: Organic Products Technology
Lecturer: Professor Stepan Melnyk, Associate Professor Anatoliy Ludyn
Semester: 7 семестр
Mode of study: денна
Мета вивчення дисципліни: teaching students about the procedure for design documentation of developing equipment and the organization of construction and installation works, designing equipment, pipelines, and workshop structures, structural features and operation principles of organic synthesis manufacture apparatuses, basics of technological calculation and apparatus layout principles.
Завдання: General competences: 1. Knowledge and understanding of the subject area and professional activity. 2. The ability to communicate orally and in writing in the national language. 3. The efforts to preserve the environment. Professional competences: 1. The ability to design chemical processes considering technical, legislative, and environmental constraints. 2. The ability to use modern materials, technologies, and apparatus designs in chemical engineering. 3. The ability to use professional knowledge and practical skills to solve specific tasks in organic substances' basic and fine synthesis technologies.
Learning outcomes: • Correctly use terminology based on the concept of chemistry, chemical technologies, processes, and equipment for manufacturing chemical substances and materials in professional activities. • To develop and implement projects related to technologies and equipment of chemical industries, taking into account goals, resources, existing constraints, social and economic aspects, and risks. • To understand the fundamental properties of structural materials and the principles and limitations of their application in chemical engineering. • To use modern computer equipment, specialized software, and information technologies to solve complex problems and practical problems in chemical engineering, particularly for calculations of equipment and processes of chemical manufacture. • To ensure the personnel and the environment safety during professional activity in chemical engineering.
Required prior and related subjects: prerequisites: prerequisites: • Chemistry and technology of organic substances • Organic synthesis processes calculation requisites • Chemical technology and engineering (course project)
Summary of the subject: The principles of developing design documentation for chemical equipment and organization of construction and installation work, features of designing devices and pipelines are outlined; properties of materials for the manufacture and protection of equipment; structural features and principles of operation of organic synthesis reactors, principles of technological calculation of reaction apparatus based on the data of operating plants, principles of design of workshop structures are considered; features of technological equipment layout.
Опис: Specificity of the equipment of organic synthesis plants. Design of technological equipment. Materials for production and protection of equipment. Thermal insulation for apparatus and pipelines. Structural features of technological equipment. Requirements for chemical reactors. Classification and application of the reaction apparatus. Principles of construction of the reactors. Reactors for gas-phase processes on the solid catalyst. Reactors for gas-phase processes using liquid catalysts. Reactors for processes in the liquid phase. Reactors for gas-phase processes. Tubular furnaces. High-pressure apparatus. Equipment for the polymerization processes. Calculation of the size of technological apparatus according to existing plants. Technology calculation of polymerization reactors Columns. Heat exchangers. Containers. Development of technological scheme. Mechanization of transport and labor-intensive work. Waste removing. Craft materials handling equipment. Overview of pipeline systems. Composition of pipeline systems. Classification of valves. Selection of pipes and valves when designing chemical plants. Features of the installation and operation of pipelines. Fundamentals of sanitary appliances. Design of industrial buildings. Industrial shelving and open areas. Personal space. Description of premises included in the structure of production. Placing the technological equipment. The principles of grouping. The main requirements when building equipment.
Assessment methods and criteria: Performance and defense of control and calculation-graphic exercises, oral and written examination, test control.
Критерії оцінювання результатів навчання: • graphical-calculation work, written express control, tests, oral questioning (30%) • final control (exam): written-oral form (70%)
Порядок та критерії виставляння балів та оцінок: 100-88 points - certified with an “excellent” grade - High level: the student demonstrates an in-depth mastery of the conceptual and categorical apparatus of the discipline, systematic knowledge, skills and abilities of their practical application. The mastered knowledge, skills and abilities provide the ability to independently formulate goals and organize learning activities, search and find solutions in non-standard, atypical educational and professional situations. The applicant demonstrates the ability to make generalizations based on critical analysis of factual material, ideas, theories and concepts, to formulate conclusions based on them. His/her activity is based on interest and motivation for self-development, continuous professional development, independent research activities, implemented with the support and guidance of the teacher. 87-71 points - certified with a grade of “good” - Sufficient level: involves mastery of the conceptual and categorical apparatus of the discipline at an advanced level, conscious use of knowledge, skills and abilities to reveal the essence of the issue. Possession of a partially structured set of knowledge provides the ability to apply it in familiar educational and professional situations. Aware of the specifics of tasks and learning situations, the student demonstrates the ability to search for and choose their solution according to the given sample, to argue for the use of a particular method of solving the problem. Their activities are based on interest and motivation for self-development and continuous professional development. 70-50 points - certified with a grade of “satisfactory” - Satisfactory level: outlines the mastery of the conceptual and categorical apparatus of the discipline at the average level, partial awareness of educational and professional tasks, problems and situations, knowledge of ways to solve typical problems and tasks. The applicant demonstrates an average level of skills and abilities to apply knowledge in practice, and solving problems requires assistance, support from a model. The basis of learning activities is situational and heuristic, dominated by motives of duty, unconscious use of opportunities for self-development. 49-00 points - certified with a grade of “unsatisfactory” - Unsatisfactory level: indicates an elementary mastery of the conceptual and categorical apparatus of the discipline, a general understanding of the content of the educational material, partial use of knowledge, skills and abilities. The basis of learning activities is situational and pragmatic interest.
Recommended books: 1. Мельник, С. Р., Мельник, Ю. Р., Піх З. Г. Проектування та розрахунок технологічних процесів органічного синтезу. Навчальний посібник – Львів: Видавництво НУ “Львівська політехніка”, 2005. – 448с. 2. Лудин А. М. Компонування технологічного обладнання: навчальний посібник / А. М. Лудин. – Львів: Левада, 2022. – 160 c. 3. Мельник С. Р., Мельник Ю. Р. Розрахунок процесів органічного синтезу: Навчальний посібник. – Львів: Видавництво «Левада», 2022. – 150 с. 4. Устаткування і основи організації виробництв тонкого органічного синтезу: Підручник / Г.А. Галстян, А.Г. Галстян, Г.О. Маршалок. – Луганськ: Вид-во «Ноулідж», 2012. – 453 с.